Peptide Orientation Affects Selectivity in Ion-Exchange Chromatography

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Peptide Orientation Affects Selectivity in Ion-Exchange Chromatography

Here we demonstrate that separation of proteolytic peptides, having the same net charge and one basic residue, is affected by their specific orientation toward the stationary phase in ion-exchange chromatography. In electrostatic repulsion-hydrophilic interaction chromatography (ERLIC) with an anion-exchange material, the C-terminus of the peptides is, on average, oriented toward the stationary...

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ژورنال

عنوان ژورنال: Analytical Chemistry

سال: 2010

ISSN: 0003-2700,1520-6882

DOI: 10.1021/ac100651k